a more complete list is available at this page :
#Mestrenova nmr manual
Here is a reference manual for CMC-assist (pdf) - not really required to read it.Ĩ.1 Shigemi & Wilmad matched insert color code SolventĨ.2 Reference compounds for chemical shift Go to the following page : Bruker Fast-Lane, to have a complete description to work with CMC-assist ISBN: 978-2-0ħ.1 CMC-assit Fast Lane on Bruker automatic machines (nmr3404l, nmr4313l & r and nmrf492l) Essential Practical NMR for Organic Chemistry John Wiley and Sons: United Kingdom, 2011 157-159. It is always the chemist at the end that has to decide if the spectra is good or not.Ī good reference for structure elucidation : Richards, S. These tools are not intended to replace the chemist but only to support him. A second soft is MestreNova Verify and is an add-on to Mestre (see 7.2). A first soft is included in ICONNMR on the automatic NMR machines (see 7.1) and does not requires installation on the user machine. ISIC has bought two softwares/licenses dedicated to help users to evaluate the consistency of their spectra. This will also suppress them on the spectrometer.įinally, in FileZilla, erase your connexion data using the small arrow on right of "connexion rapide" and clicking on "effacer historique". Your USB key should be visible in the left window under "Volume" folder.ĭata are available on the right window under path : /spectro/MACHINE/guests/data/USER/nmrĬopy all data simply by drag and drop from server to your key, then suppress all data on the server. The right window in FileZilla is the remote machine (server) and the left window is the local machine.
#Mestrenova nmr password
G13000, G has to be capital) and you password (port 21 = FTP mode). This machine is equipped with FileZillaĬonnect yourself to the server using FileZilla, connexion information are host =, user = USER (e.g.
#Mestrenova nmr mac
This will generate data into the following folder : /opt/data/guests/data/USER/nmr/.Ī dedicated MAC machine is available in the BCH 1512 room.
In TOPSPIN or XWINNMR, type "EDC" or "NEW", in the popup window fill the following information :ĭIR type : /opt/data/guests (this folder is in mode 770, root : 500000) The two dedicated machines for external users are nmr1512l and nmr1512r. NMR service can not be considered as responsible in case of loss or diffusion of data that have not been correctly removed from the spectrometer by external/guests users. We therefore ask GUESTS users to directly retrieve their data after acquisition and to erase them from the spectrometer (see 2.2.2).ĭedicated folders are specifically not backed-up. It is also possible to connect directly to the server using the drive mapping process, see below.įor confidentiality reasons, we do not store nor backup any external user data. You can therefore drag them in your computer (left window, blue). In the right window (red one, server) choose the spectro link, then choose the correct spectrometer. Then connect with the following information: This will avoid any modification of the files during the file transfer. In the upper window (Default Transfer Type) choose the "Binary" option. Good sensitivity in 13C and 31P.ĭedicated to short terms experiments FileTypes options. Yes (prodigy, N 2) factor 2 in sensitivityĪUTOMAT,very good sensitivity in 1H and 19F. Good routine machine for 1H, 13C, 19F and 31P.ĪUTOMAT, high sensitivity in 1H, 19F, 13C and 31P, good for characterization. !! GOOD for 1H (zg and COSY) and all reverse experimet Special machine for high pressure measurments Good routine machine for 1H, 13C, 19F and 31P !! IDEAL for low concentrated 13C samples !! IDEAL for 1H (zg and COSY) and all reverse experiments such HSQC and HMQC. Short to medium experiments for NMR routine 13C samples - Prefer CryoProbes in this caseġH,, very good sensitivity on proton, simple gradient, medium sensitivity on broad band. !! T° limit 0☌ to 60☌ (due to the cryoprobe)ġH, 13C, BB, good sensitivity on carbon and other low gamma nuclei such as 31Pġ5 N, 51 V, 11B are accessible on this machine Liquid: High resolution, low concentration samples (bio)
!! T° limit 0☌ to 80☌ (due to the cryoprobe) Table of Signal to Noise ratio © Martial Rey Table of all available probes and machines at epfl © Martial Rey Routine TOPSPIN commands for manual machine Available NMR spectrometers and ideal useĤ. If you need some complement, do not hesitate to contact us at pascal.mieville"at"epfl.ch.ġ. We hope you will find here answers to your questions regarding the NMR service of the Institut des Sciences et Ingénieurie Chimiques de l'EPFL.
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